02 March 2017

This is the sample log

  • test: NV are on the depth of about 20um, no shallow NV
  • ICP long time (recipe: Ar/Cl2 160W 200W 30min * 12times real depth = 10.11um) follows piranha clean
  • test: surface is a slope - unable to determine surface position; surface is dirty
  • ICP (recipe: O2-7/Ar-8 normal) follows piranha clean
  • test: surface is still bad (slope even broader), no NV in proper depth
  • ICP (recipe: O2-7/Ar-8 normal) follows piranha clean
  • test: the same as ICP before
  • ICP (recipe: Ar/Cl2 200W 320W 1. 1h real_depth=2.5um 2. 2h real_depth=5.65um total_depth=8.58um) follows piranha clean
  • Piranha, Evaporate Al 20nm
  • adhere sample to stage by colloidal silver and bake 30min at 110°C
  • FIB chipname and markers (700um*700um)
  • remove Al and colloidal silver
  • NV location (found 10)
  • NV spectrum testing (Chang Xiuying)


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